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Microwave synthesis equipment - List of Manufacturers, Suppliers, Companies and Products

Microwave synthesis equipment Product List

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Microwave reaction

Our company conducts various reactions using microwave synthesis equipment!

Microwaves are a type of electromagnetic wave, and when microwaves are irradiated, they are absorbed by a substance depending on its dielectric properties, causing the substance itself to heat up. This phenomenon is utilized as a new heat source for organic synthesis reactions. Due to the wide variety of applicable reactions, our company conducts various reactions using microwave synthesis equipment. **Effects of Microwaves** - Reduction of reaction time, suppression of side reactions, and improvement of yields are possible. - Since it acts directly on the substance, it allows for solvent-free reactions, uniform heating in solid-phase reactions, and promotes reactions. - The ability to conduct reactions at temperatures higher than the boiling point leads to effects such as improved solubility. - Microwave-specific effects such as positional selectivity, stereoselectivity, and high crystallization. *For more details, please refer to the related link page or feel free to contact us.*

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Free test exam available: 'Flow-type microwave synthesis device'

Maximum temperature 230℃, maximum pressure 2.5MPa! Heating efficiency improved by unique microwave control technology! Usable from research to production processes in a tabletop size.

The "Flow-Type Microwave Synthesis Device" is a system that allows for efficient heating through our company's developed glass reaction tube (coil). It is a compact size that can be operated on a desk, enabling a smooth transition from research to production processes. 【Features】 ■ Improved efficiency through our unique microwave control technology ■ Reduced reaction time due to uniform and rapid heating ■ High reproducibility through uniform heating and continuous chemical reactions ■ Increased yield due to uniform heating and high reproducibility ■ High safety due to a compact reaction space ■ Significant cost reduction through automation *For more details, please download the PDF or feel free to contact us.

  • Other physicochemical equipment
  • Heating device

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Example of reaction: Claisen rearrangement reaction

Introducing the reaction results using a flow-type microwave synthesis device in detail!

Our "flow-type microwave synthesis device" can heat the entire system while flowing the target substance (liquid) through a glass serpentine tube, eliminating the need for multiple heating steps and enabling uniform heating. Using this device, we will introduce the reaction results and experimental methods for the synthesis of 2-allylphenol via a Claisen rearrangement reaction using allyl phenyl ether as the starting material. 【Overview】 ■ Under the conditions of microwave output 100W and flow rate 0.5 mL/min, using N,N-dimethylformamide (DMF) as the reaction solvent (applied pressure ca. 1.7 MPa, ca. 290℃), the progress of the reaction was confirmed by TLC analysis, and the chemical structure of the product was determined by NMR analysis. ■ As a result, the disappearance of the starting material was confirmed, and the desired 2-allylphenol was obtained as the main product. *For more details, please refer to the PDF document or feel free to contact us.

  • Other physicochemical equipment
  • Heating device

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Fisher-Indole Synthesis

We will provide a detailed introduction to the reaction results using a flow-type microwave synthesis device!

Our "flow-type microwave synthesis device" can heat the entire system while flowing the target substance (liquid) through a glass serpentine tube, eliminating the need for multiple heating steps and allowing for uniform heating. Using this device, we will introduce the reaction results of producing tetrahydrocarbazole through the Fischer indole synthesis reaction of phenylhydrazine and cyclohexanone, as well as the experimental methods. [Overview] ■ Production of tetrahydrocarbazole through the Fischer indole synthesis reaction of phenylhydrazine and cyclohexanone. *For more details, please refer to the PDF document or feel free to contact us.

  • Other physicochemical equipment
  • Heating device

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Diels-Alder reaction

A detailed introduction to the reaction results using a flow-type microwave synthesis device!

Our "flow-type microwave synthesis device" can heat the entire system while flowing the target substance (liquid) through a glass coil, eliminating the need for multiple heating steps and allowing for uniform heating. We will introduce the Diels-Alder reaction of furan and acetylene dicarboxylate using this device, as well as the experimental methods. 【Overview】 ■ Diels-Alder reaction of furan and acetylene dicarboxylate *For more details, please refer to the PDF document or feel free to contact us.

  • Other physicochemical equipment
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Example of Reaction: Fisher Ester Synthesis

We will provide a detailed introduction to the reaction results using a flow-type microwave synthesis device!

Our "flow-type microwave synthesis device" can heat the entire system while flowing the target substance (liquid) through a glass coil, eliminating the need for multiple heating steps and allowing for uniform heating. We will introduce the Fischer esterification reaction of benzoic acid using this device, as well as the experimental methods. [Overview] ■ Fischer esterification reaction of benzoic acid *For more details, please refer to the PDF document or feel free to contact us.

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Microwave Synthesis Device "Discover 2.0"

Single-mode microwave synthesis device utilizing the latest technology.

"Discover 2.0" is the ultimate microwave reactor for all organic and inorganic synthesis experiments. It features a class-leading 300 mL single-mode microwave cavity and an intuitive software with a 10-inch touchscreen interface, allowing you to program reactions in seconds and achieve the best synthesis yields in minutes. 【Features】 ■ The most extensive pressurized sealed containers for single-mode microwave synthesis – 10mL, 35mL, 100mL ■ Infrared temperature sensor (iWave) that can see through glass and Teflon ■ Technology for safely venting excessive pressure and resealing (Activent) ■ Variable-speed magnetic stirring function and rapid cooling with compressed air ■ Upgrade options: 12/24 position automatic sampler, gas introduction device, simultaneous cooling module (-80℃ and below), flow cell

  • Company:CEM Japan
  • Price:1 million yen-5 million yen
  • Other physicochemical equipment

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Reaction example: Suzuki - Miura coupling

Introducing examples of experiments using a flow-type microwave synthesis device!

Our "flow-type microwave synthesis device" can heat the entire system while flowing the target substance (liquid) through a glass serpentine tube, eliminating the need for multiple heating steps and allowing for uniform heating. We will introduce examples of experiments using this device, along with corresponding batch reaction experiments. [Overview] ■ After all raw materials are completely dissolved, nitrogen gas is bubbled for 5 minutes through a Pasteur pipette. ■ The supply of the cleaning solution for the device's flow path (DME:EtOH 1:1) is started, and microwaves are irradiated while waiting for the temperature to stabilize. ■ NMR measurements of the obtained mixture are conducted to calculate the yield of the product and the recovery rate of the raw materials. *For more details, please refer to the PDF document or feel free to contact us.

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Aromatic nucleophilic substitution reaction

We will introduce the reaction results using a flow-type microwave synthesis device in detail!

Our "flow-type microwave synthesis device" can heat the entire system while flowing the target substance (liquid) through a glass coil, eliminating the need for multiple heating steps and allowing for uniform heating. We will introduce the nucleophilic substitution reaction of nitro dichlorobenzene and the experimental methods using this device. [Overview] ■ Nucleophilic substitution reaction of nitro dichlorobenzene *For more details, please refer to the PDF document or feel free to contact us.

  • Other physicochemical equipment
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Flow-type microwave synthesis device

Safety mechanism linked to temperature and pressure sensors! Introduction to the microwave synthesis device.

The "Flow-type Microwave Synthesis Device" is a microwave device for continuous flow synthesis. The feature of this device is its uniform and rapid microwave heating of the flow channel. Therefore, it not only introduces a new heating method for continuous flow synthesis but also contributes to the scale-up of microwave synthesis, which has been difficult with batch-type microwave devices. Furthermore, this system provides a synthesis environment of up to 230°C and a maximum pressure of 2.5 MPa. We support our customers with the microwave and flow technologies and expertise we have cultivated so far. [Features] - Dedicated design for flow - Uniform and rapid microwave heating of the flow channel - High temperature and high pressure (up to 230°C & 2.5 MPa) environment - Safety mechanisms linked to temperature and pressure sensors - Lineup of reaction tubes for flow synthesis, including those for solid catalysts *You can download the English version of the catalog. *For more details, please refer to the PDF document or feel free to contact us.

  • High frequency/microwave parts

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